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What are the effects of storm? Study Guides. Trending Questions. Still have questions? Find more answers. Previously Viewed. Errors may be present in: - the design of the experiment. Preparing Solutions of Precise Concentration It is often necessary to prepare solutions of precisely known concentration of a substance If the substance. Measurement Notes Chapter 2 Length Scientist use the metric system—a standard measurement system based on the The meter is the basic unit.
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Presentation is loading. Please wait. Copy to clipboard. Presentation on theme: "Why Weigh by Difference? Analytical balances can. Download ppt "Why Weigh by Difference? CHM About project SlidePlayer Terms of Service. Now to my knowledge would this not increase the uncertainty as instead of just using the beaker on the scale and adding the mass directly which would lead to one uncertainty we instead weigh it twice which would thus have 2x the uncertainty in the scale.
Although there are several sources of weighing error that would be minimized by using the weighing by difference method as discussed in the comments , I want to illustrate what I see as the limiting problem, that of the relative uncertainty of the measurement, which roughly scales no pun intended, really with the mass being measured.
Lets use a bit of an exaggerated situation for illustration. In reality you would likely have a high-mass balance for weighing directly into the beaker, or a low-mass balance for using the weighing boat. We are just using one really good balance to simplify this illustration, but the concept is the same either way. So, even with two measurements rather than one, using the weighing boat method results in much less total uncertainty in the measured mass of your material as compared to weighing a small quantity of material directly into a large beaker.
Most chemists in the lab I have seen so far caution: sample distribution may be skewed usually do not reweigh whatever they weighed into after transferring into the reaction vessel or beaker. For most substances, this is justifyable since you can see if significant bits remain in the boat or weighing device you used. In rare cases, especially when I see lots of a substance remaining, I will reweigh the boat or weighing vessel, though.
As to the question of weighing into a boat or the beaker this is more complicated. For one, the uncertainty usually increases roughly linearly with the weight of the sample measured. The smaller and lighter the vessel you use, the less it affects the total weight on the scales and thus also the less inaccurate your weighing is. Weighing directly into the beaker or flask can also have practical disadvantages.
If — what is often the case in synthesis — you need to weigh more than one compound, you should keep them separate in the weighing step since you will probably have to add and remove to get to the mass you want to have. Furthermore, these reaction vessels typically allow for a somewhat easy addition of solids into them, but make it very hard to remove a bit of solid from them, e.
These problems come on top of the scaling uncertainty, making weighing directly into a flask more and more unsuitable. Sign up to join this community.
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